Please use this identifier to cite or link to this item: http://repositorio.unitau.br/jspui/handle/20.500.11874/2373
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dc.contributor.authorRichetto K.C.S.pt_BR
dc.contributor.authorSilva C.R.M.pt_BR
dc.contributor.authorBaldacin S.A.pt_BR
dc.date.accessioned2019-09-12T16:37:10Z-
dc.date.available2019-09-12T16:37:10Z-
dc.date.issued2003-
dc.citation.volume416-418pt_BR
dc.citation.issue1pt_BR
dc.citation.spage688-
dc.citation.epage692-
dc.identifier.issn2555476-
dc.identifier.urihttps://www.scopus.com/inward/record.uri?eid=2-s2.0-0037285535&partnerID=40&md5=4e0b7053d7af97285fb022be55e375b7-
dc.identifier.urihttp://repositorio.unitau.br/jspui/handle/20.500.11874/2373-
dc.description.abstractSilicon nitride powder synthesis, performed by silicon tetrachloride ammonolysis, is described in this work. Gaseous ammonia reacts with liquid SiCl4, at low temperature and inert atmosphere. At a second step, a powder pyrolysis of silicon diimide is performed between 1300 and 1500°C, for ammonium chloride removal and Si3N4 formation. Phase formation is evaluated by X-ray diffraction. Particle medium size and form is determined by Scanning Electron Microscopy.en
dc.description.provenanceMade available in DSpace on 2019-09-12T16:37:10Z (GMT). No. of bitstreams: 0 Previous issue date: 2003en
dc.languageInglêspt_BR
dc.relation.ispartofMaterials Science Forum-
dc.rightsAcesso Restritopt_BR
dc.sourceScopuspt_BR
dc.subject.otherQualitative analysisen
dc.subject.otherSilicon nitrideen
dc.subject.otherSynthesisen
dc.subject.otherAmmonium chlorideen
dc.subject.otherAmmonolysisen
dc.subject.otherPhase formationen
dc.subject.otherPowder pyrolysisen
dc.subject.otherQualitative analysisen
dc.subject.otherSilicon diimideen
dc.subject.otherSilicon tetrachlorideen
dc.subject.otherAmmoniaen
dc.subject.otherAmmonium compoundsen
dc.subject.otherChlorine compoundsen
dc.subject.otherLiquidsen
dc.subject.otherOrganic solventsen
dc.subject.otherPhase transitionsen
dc.subject.otherPowdersen
dc.subject.otherPyrolysisen
dc.subject.otherScanning electron microscopyen
dc.subject.otherSynthesis (chemical)en
dc.subject.otherTemperatureen
dc.subject.otherX ray diffraction analysisen
dc.subject.otherSilicon nitrideen
dc.titleQualitative analysis of silicon nitride synthesized by ammonolysis of silicon tetrachlorideen
dc.typeArtigo de Periódicopt_BR
dc.description.affiliationRichetto, K.C.S., UNITAU - Universidade de Taubate, Taubate, SP, Brazil-
dc.description.affiliationSilva, C.R.M.-
dc.description.affiliationBaldacin, S.A.-
dc.identifier.scopus2-s2.0-0037285535-
dc.contributor.scopus7801505879pt_BR
dc.contributor.scopus25931164300pt_BR
dc.contributor.scopus35333507000pt_BR
Appears in Collections:Artigos de Periódicos

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